4-Pyridinepropanol → HCID 54209077, compound

HRID 392698Notes

Reaction equation

[C:1]1([CH:7]([C:13]2[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=2)[C:8]([N:10]=[C:11]=[O:12])=[O:9])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[N:19]1[CH:24]=[CH:23][C:22]([CH2:25][CH2:26][CH2:27][OH:28])=[CH:21][CH:20]=1>>[N:19]1[CH:24]=[CH:23][C:22]([CH2:25][CH2:26][CH2:27][O:28][C:11](=[O:12])[NH:10][C:8](=[O:9])[CH:7]([C:1]2[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=2)[C:13]2[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=2)=[CH:21][CH:20]=1

Participants

Reactant 2

HCID 729234-Pyridinepropanol

HCID 11264874Diphenylacetyl isocyanate

Product 1

HCID 54209077HCID 54209077, compound

Procedure

The title compound, brown solid, m.p. 147-50° C. and MS: m/e=374.4 (M+H+) was prepared in accordance with the general method of example 1 from diphenylacetyl isocyanate and 3-pyridin-4-yl-propan-1-ol.

Sources & evidence

ORD record: ord-b553d5355257453bacff5212963f5d31
Source dataset: uspto-grants-2004_10
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US06803381B1

Reaction notes

Loading…