9H-xanthene-9-carbonyl chloride → HCID 54186208, compound

HRID 392746Notes

Reaction equation

HRID 392746 reaction equation
[CH:1]1([C:4]2[N:8]=[C:7]([NH2:9])[O:6][N:5]=2)[CH2:3][CH2:2]1.[CH:10]1[C:23]2[CH:22]([C:24](Cl)=[O:25])[C:21]3[C:16](=[CH:17][CH:18]=[CH:19][CH:20]=3)[O:15][C:14]=2[CH:13]=[CH:12][CH:11]=1>>[CH:1]1([C:4]2[N:8]=[C:7]([NH:9][C:24]([CH:22]3[C:23]4[CH:10]=[CH:11][CH:12]=[CH:13][C:14]=4[O:15][C:16]4[C:21]3=[CH:20][CH:19]=[CH:18][CH:17]=4)=[O:25])[O:6][N:5]=2)[CH2:3][CH2:2]1

Participants

3

Reactant 2

HCID 27608929H-xanthene-9-carbonyl chlorideHCID 226610563-Cyclopropyl-1,2,4-oxadiazol-5-amine

Product 1

HCID 54186208HCID 54186208, compound

Procedure

The title compound, white solid, m.p. 275° C. and MS: m/e=333 (M+) was prepared in accordance with the general method of example 44a from 3-cyclopropyl-[1,2,4]oxadiazol-5-ylamine and 9H-xanthene-carboxylic acid chloride.

Sources & evidence

ORD record
ord-d43accdcd13b4be4871c14e338f77c1f
Source dataset
uspto-grants-2004_10
Patent number
US06803381B1

Reaction notes

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