HuagongsheHuagongshe Chemistry Print Report · For research reference only
3,4-Dichloroaniline → HCID 693064, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3,4-Dichloroaniline | HCID 7257 | — |
| Reactant | 4-Fluorobenzoyl chloride | HCID 67879 | — |
| Product | HCID 693064 | HCID 693064 | — |
Reaction Steps
Reaction of 4-fluorobenzoyl chloride with 3,4-dichloroaniline using Method II, step 1, gave the title amide as crystals: mp 160-161° C. (ethyl acetate-hexane). 1HNMR 400 MHz (CDCl3) δ (ppm): 7.19 (2H, m, aromatics), 7.44 (2H, m, aromatics), 7.70 (1H, broad, NH), 7.88 (3H, m, aromatics). Anal. Calcd for C13H18Cl2FNO: C, 54.96; H, 2.84; N, 4.93. Found: C, 54.96; H, 2.87; N, 4.90.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06803378B2 |
| Source dataset | uspto-grants-2004_10 |
| ORD ID | ord-d30041f089b2416a9f1ba66641a7e96e |
| Source note | uspto-grants-2004_10 |