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HRID392946

反应详情

EQUATION

反应方程式

HRID 392946 的结构方程式

REACTANTS

反应物

3
结构：O=S(Cl)Cl
HCID24386

Thionyl chloride

Cl2OS

结构：CCO[Si](OCC)(c1c(F)c(F)c(F)c(F)c1F)c1c(F)c(F)c(F)c(F)c1F
HCID11102434

未命名化合物

结构：Cl.c1cc[nH+]cc1
HCID21584435

未命名化合物

PRODUCTS

生成物

1
结构：Fc1c(F)c(F)c([SiH](OCCCl)c2c(F)c(F)c(F)c(F)c2F)c(F)c1F
HCID131724616

未命名化合物

PROCEDURE

实验过程

180.93 g (0.400 mol) di(pentafluorophenyl)diethoxysilane, 29 mL (0.400 mol, 47.6 g) thionylchloride and 4.92 g (0.0426 mol) pyridinium hydrochloride are refluxed and stirred for 16 h. Unreacted SOCl2 is evaporated and di(pentafluorophenyl)chloroethoxysilane isolated by vacuum distillation.

WORKUP

后处理

  1. customUnreacted SOCl2 is evaporated