HuagongsheHuagongshe Chemistry Print Report · For research reference only
Propargyl alcohol → HCID 13008219, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Propargyl alcohol | HCID 7859 | — |
| Reactant | HCID 13008218 | HCID 13008218 | — |
| Catalyst | Copper(1+) iodide; Copper(I) iodide; Cuprous iodide; Cuprous iodide (CuI) | HCID 24350 | — |
| Solvent | Triethylamine | HCID 8471 | — |
| Product | HCID 13008219 | HCID 13008219 | — |
Reaction Steps
A schlenk tube was charged with 62.5 mg of dichlorobistriphenylphosphine palladium (II) complex and 45.5 mg of copper (I) iodide, and an atmosphere in the system was replaced with nitrogen. 31.9 Grams of p-iodobenzoic acid-(R)-3-ethyl-1-methylpentyl ester and 7.50 g of 2-propyn-1-ol were dissolved in 100 mL of dry triethylamine, and the mixture was charged into the above schlenk tube and stirred at room temperature for 1 day.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06805921B2 |
| Source dataset | uspto-grants-2004_10 |
| ORD ID | ord-1b67df47852440a5930e504a8a007445 |
| Source note | uspto-grants-2004_10 |