5-Benzyloxy-alpha,alpha,alpha',alpha'tetramethyl-1,3-benzenedimethanol → 3,5-Bis(1-ethylpropyl)phenol

HRID 393406Notes

Reaction equation

HRID 393406 reaction equation
C(OC1C=C(C(C)(C)O)C=C(C(C)(C)O)C=1)C1C=CC=CC=1.C([O:30][C:31]1[CH:32]=[C:33]([C:43]([CH2:47][CH3:48])([CH2:45][CH3:46])O)[CH:34]=[C:35]([C:37]([CH2:41][CH3:42])([CH2:39][CH3:40])O)[CH:36]=1)C1C=CC=CC=1>>[CH2:45]([CH:43]([C:33]1[CH:32]=[C:31]([OH:30])[CH:36]=[C:35]([CH:37]([CH2:39][CH3:40])[CH2:41][CH3:42])[CH:34]=1)[CH2:47][CH3:48])[CH3:46]

Participants

3

Reactant 2

HCID 99223705-Benzyloxy-alpha,alpha,alpha',alpha'tetramethyl-1,3-benzenedimethanolHCID 226603395-Benzyloxy-alpha,alpha,alpha',alpha'-tetraethyl-1,3-benzenedimethanol

Product 1

HCID 226603373,5-Bis(1-ethylpropyl)phenol

Procedure

The procedure (including reaction and treatment) of Example 2 was repeated, except that 5-benzyloxy-α,α,α′,α′tetramethyl-1,3-benzenedimethanol was replaced by 5-benzyloxy-α,α,α′,α′-tetraethyl-1,3-benzenedimethanol, to thereby yield the above-described target as colorless needles.

Workup

  1. customThe procedure (including reaction and treatment) of Example 2
  2. customto thereby yield the above-described target as colorless needles

Sources & evidence

ORD record
ord-77afbfa2f1df4817b3f2aa13e3c9f895
Source dataset
uspto-grants-2004_10
Patent number
US06806395B2

Reaction notes

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