HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Bromonaphthalene → HCID 10944814, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Bromonaphthalene | HCID 11372 | — |
| Reactant | 1-Bromo-4-nitrobenzene | HCID 11466 | — |
| Catalyst | Copper | HCID 23978 | — |
| Product | HCID 10944814 | HCID 10944814 | — |
Reaction Steps
202 g of 1-bromo-4-nitrobenzene and 207 g of 2-bromonaphthalene were subjected to Ullmann coupling using a copper catalyst. The product was purified by a column chromatography to obtain 2-(4-nitrophenyl)naphthalene. The product was reduced using a reduced iron to obtain 2-(4-aminophenyl)naphthalene (yield: 36%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06808869B1 |
| Source dataset | uspto-grants-2004_10 |
| ORD ID | ord-df32556364fe42828707ae52096e45f6 |
| Source note | uspto-grants-2004_10 |