HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → Ethyl 3-[4-[2-(2,3-dihydro-1,4-benzoxazin-4-yl)ethoxy]phenyl]-2-butoxypropanoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 2-(2,3-Dihydro-1,4-benzoxazin-4-yl)ethyl methanesulfonate | HCID 10422590 | — |
| Reactant | Ethyl 2-butoxy-3-(4-hydroxyphenyl)propanoate | HCID 21930975 | — |
| Product | Ethyl 3-[4-[2-(2,3-dihydro-1,4-benzoxazin-4-yl)ethoxy]phenyl]-2-butoxypropanoate | HCID 9910403 | 52.6% |
Reaction Steps
The title compound (0.4 g, 52%) was prepared as a gummy liquid from 2-(2,3-dihydro-1,4-benzoxazin-4-yl)ethyl methanesulfonate (0.46 g; 1.78 mmol), potassium carbonate (0.98 g, 7.12 mmol) and ethyl 2-butoxy-3-(4-hydroxyphenyl)propanoate (0.47 g, 1.78 mmol) using conditions analogous to that described in preparation 2.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06809095B2 |
| Source dataset | uspto-grants-2004_10 |
| ORD ID | ord-9b72b01a038544da99317ce10f55cd77 |
| Source note | uspto-grants-2004_10 |