HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl 4-[(acetylsulfanyl)methyl]oxane-4-carboxylate → 1-Acetylsulfanylmethylcyclohexanecarboxylic acid methyl ester
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl 4-[(acetylsulfanyl)methyl]oxane-4-carboxylate | HCID 23448262 | — |
| Reactant | Methyl 1-(iodomethyl)cyclohexanecarboxylate | HCID 58947958 | — |
| Product | 1-Acetylsulfanylmethylcyclohexanecarboxylic acid methyl ester | HCID 58947950 | 92% |
Reaction Steps
Prepared according to the method for the preparation of 4-acetylsulfanylmethyltetrahydropyran-4-carboxylic acid methyl ester, from 1-iodomethylcyclohexanecarboxylic acid methyl ester (20 g), to yield the title compound as a brown gum (15 g, 92%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06809100B2 |
| Source dataset | uspto-grants-2004_10 |
| ORD ID | ord-f1fc7002919e45578ab70aacfdbdf934 |
| Source note | uspto-grants-2004_10 |