HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Bromo-5-methoxypyridine → HCID 23636153, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Bromo-5-methoxypyridine | HCID 817163 | — |
| Reactant | benzyl (1S,5S)-3,6-diazabicyclo[3.2.0]heptane-3-carboxylate | HCID 23635906 | — |
| Product | HCID 23636153 | HCID 23636153 | 37% |
Reaction Steps
The product of Example 52D (940 mg, 4.05 mmol) and 3-bromo-5-methoxypyridine (1.13 g, 6.07 mmol) were processed according to the procedure described in Example 1E. The crude product was purified by chromatography (SiO2, ethyl acetate:hexane, 1:1) to provide the title compound (0.50 g, 37% yield). MS (DCI/NH3) m/z 340 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06809105B2 |
| Source dataset | uspto-grants-2004_10 |
| ORD ID | ord-b4e3df9806da4949ad0d3a2b4ae0517a |
| Source note | uspto-grants-2004_10 |