HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 15505944, compound → HCID 15505947, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 15505944 | HCID 15505944 | — |
| Reactant | Sodium 1,4-bis[(2-ethylhexyl)oxy]-1,4-dioxobutane-2-sulfonate--1,8-dihydroxyanthracene-9,10-dione (1/1/1) | HCID 23675773 | — |
| Solvent | Chlorobenzene | HCID 7964 | — |
| Product | HCID 15505947 | HCID 15505947 | 53% |
Reaction Steps
The synthesis was carried out essentially as described for 2a, but chlorobenzene was used as a solven instead of methylene chloride. Yield: 53%. Found: C, 83.84; H, 4.69; C29H20O3 (MW 416.47) requires C, 83.63; H, 4.84%. Mass-spectrum, MALDI-TOF: 416.92 (100), 252.65 (60). Calculated exact mass for C29H20O3:416.14125; found 416.14125.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06809220B2 |
| Source dataset | uspto-grants-2004_10 |
| ORD ID | ord-d668b89b72774ea595966c2d22b8e9f7 |
| Source note | uspto-grants-2004_10 |