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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 39404Erstellt: 25. Oktober 2026

HCID 21134990, Verbindung → HCID 67607843, Verbindung

https://huagongshe.com/reaction/39404

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktHCID 21134990HCID 21134990—
Edukt2-methyl-1-phenylpropan-2-yl 2-((4R,6S)-6-(chloromethyl)-2,2-dimethyl-1,3-dioxan-4-yl)acetateHCID 67607702—
ProduktHCID 67607843HCID 67607843—

Reaktionsschritte

The procedure was carried out in the same manner as in Example 11, except that 3.5 g of 2-methyl-1-phenylpropan-2-yl 2-((4R,6S)-6-(chloromethyl)-2,2-dimethyl-1,3-dioxan-4-yl)acetate was used in place of 30 g thereof, and sodium 1-methyl-1H-benzo[d]imidazole-2-thiolate (3.7 g) prepared in Example 9 was used in place of sodium 1-phenyl-1H-tetrazole-5-thiolate. The title compound was obtained (4.7 g).

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS08524914B2
Quelldatensatzuspto-grants-2013_09
ORD IDord-203fa7ae779f4adf88cc967c5402530a
Quellennotizuspto-grants-2013_09