HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sulfuric Acid → 4-(Chloromethyl)-2-(4-chlorophenyl)-1,3-thiazole
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sulfuric Acid | HCID 1118 | — |
| Reactant | 1,3-Dichloroacetone | HCID 10793 | — |
| Reactant | 4-Chlorothiobenzamide | HCID 2734826 | — |
| Product | 4-(Chloromethyl)-2-(4-chlorophenyl)-1,3-thiazole | HCID 610297 | — |
Reaction Steps
In analogy to the procedure described in example 4 a], 4-chlorothiobenzamide was reacted with 1,3-dichloroacetone followed by treatment with concentrated sulfuric acid to obtain 4-chloromethyl-2-(4-chloro-phenyl)-thiazole as colorless crystals.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06809110B2 |
| Source dataset | uspto-grants-2004_10 |
| ORD ID | ord-ee9f13dfa3e24067a6276b56dbad7bb0 |
| Source note | uspto-grants-2004_10 |