HuagongsheHuagongshe Chemistry Print Report · For research reference only
Aluminium lithium hydride → 3-(2-Phenyl-thiazol-4-yl)-propan-1-ol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Aluminium lithium hydride | HCID 21226445 | — |
| Reactant | 3-(2-Phenyl-thiazol-4-yl)-propionic acid ethyl ester | HCID 68616668 | — |
| Product | 3-(2-Phenyl-thiazol-4-yl)-propan-1-ol | HCID 22647495 | 76% |
Reaction Steps
In analogy of the procedure described in example 12 b], 0.44 g (1.68 mmol) of 3-(2-phenyl-thiazol-4-yl)-propionic acid ethyl ester was reacted with lithium aluminium hydride, yielding 0.28 g of 3-(2-phenyl-thiazol-4-yl)-propan-1-ol as colorless liquid (75.8% of theory).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06809110B2 |
| Source dataset | uspto-grants-2004_10 |
| ORD ID | ord-07277705a0cd4d4985dca79089eb6c04 |
| Source note | uspto-grants-2004_10 |