HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 3352947, compound → HCID 3515208, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 3352947 | HCID 3352947 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 3515208 | HCID 3515208 | 85.1% |
Reaction Steps
N-(4-nitrobenzoyl)-2-carbomethoxypyrrolidine (0.54 g, 1.94 mmol) in MeOH (50 mL) with 10% Pd-C (0.10 g) was shaken under an atmosphere of H2 gas (50 psi) for 4 h. The reaction was filtered through a plug of Celite® and evaporated to give 0.41 g of the aniline; LRMS (M+H)+ m/z=249.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06602895B2 |
| Source dataset | uspto-grants-2003_08 |
| ORD ID | ord-b82a723f82a148d998e9a9c55b8b235e |
| Source note | uspto-grants-2003_08 |