HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetone → 2,4-BIS(ALLYLOXY)BENZALDEHYDE
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetone | HCID 180 | — |
| Reactant | 2,4-Dihydroxybenzaldehyde | HCID 7213 | — |
| Reactant | Allyl bromide | HCID 7841 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Product | 2,4-BIS(ALLYLOXY)BENZALDEHYDE | HCID 5182408 | 93% |
Reaction Steps
To a solution of 6.9 g (50 mmol) of 2,4-dihydroxybenzaldehyde in 100 ml of acetone was added 12 ml (120 mmol) of 3-bromopropene and 40 g of potassium carbonate and the mixture was refluxed for 3 h under stirring. The mixture was filtered and the filtrate concentrated in vacuo to give 10.2 g (93%) of 2,4-diprop-2-enyloxybenzaldehyde as slightly reddish crystals.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06603046B1 |
| Source dataset | uspto-grants-2003_08 |
| ORD ID | ord-b4afe83461064144a8ba926fc5539048 |
| Source note | uspto-grants-2003_08 |