Ammonium Hydroxide → HCID 69625570, compound

Participants

Reaction Steps

To a solution of 9 (5.0 mg, 0.00845 mmol) in MeOH (0.5 mL) was added NH4OH (1.5 mL). The mixture was stirred at ambient temperature for 3 hours, then concentrated in vacuo to give a crude solid. Recrystallization with MeOH/hexane/CHCl3 afforded 4.3 mg (90.5%) as a yellow solid.

Provenance & Evidence