HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 395264Generated: October 26, 2026
Hydrogen Bromide → 2,3,4,5-tetrahydro-1H-3-benzazepin-7-ol hydrobromide
https://huagongshe.com/reaction/395264
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Hydrogen Bromide | HCID 260 | — |
| Reactant | 7-Methoxy-2,3,4,5-tetrahydro-1h-3-benzazepine | HCID 13853348 | — |
| Product | 2,3,4,5-tetrahydro-1H-3-benzazepin-7-ol hydrobromide | HCID 23331391 | — |
Reaction Steps
7-Methoxy-2,3,4,5-tetrahydro-1H-3-benzazepine (10 g) in 48% aqueous hydrobromic acid (350 ml) was allowed to stir at 100° C. for 4 h. The mixture was cooled to 20° C. then evaporated to dryness in vacuo to give the title compound (14.5 g) as a brown solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US06605607B1 |
|---|
| Source dataset | uspto-grants-2003_08 |
|---|
| ORD ID | ord-06c471aa95454f4dbe946f9057bfaef9 |
|---|
| Source note | uspto-grants-2003_08 |
|---|
