HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Chloro-4-iodobenzene → 11-(4-Chlorophenyl)undec-10-yn-1-ol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Chloro-4-iodobenzene | HCID 12510 | — |
| Reactant | 10-Undecyn-1-ol | HCID 76015 | — |
| Product | 11-(4-Chlorophenyl)undec-10-yn-1-ol | HCID 22678107 | — |
Reaction Steps
In a manner described in Example 18 above, 10-undecyn-1-ol was reacted with 1-chloro-4-iodobenzene to give the title compound; NMR (CDCl3) δ 1.21-1.50 (m, 10H), 1.50-1.65 (m, 4H), 2.36-2.41 (m, 2H), 3.61-3.66 (m, 2H), 7.16-7.31 (m, 4H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06605628B1 |
| Source dataset | uspto-grants-2003_08 |
| ORD ID | ord-f4fe4d74fb564c50b9ea7cfec2fb7333 |
| Source note | uspto-grants-2003_08 |