4-Bromobiphenyl → 3-([1,1'-Biphenyl]-4-yl)prop-2-yn-1-ol

Participants

Role	Name	HCID	Charge
Reactant	4-Bromobiphenyl	HCID 7101	—
Reactant	Propargyl alcohol	HCID 7859	—
Product	3-([1,1'-Biphenyl]-4-yl)prop-2-yn-1-ol	HCID 22320753	—

Reaction Steps

In a manner described in Example 18 above, propargyl alcohol was reacted with 4-bromobiphenyl to give the title compound as white crystals: NMR (CDCl3) δ 4.53 (d, J=4.74, 2H), 7.38 (d, J=7.17, 1H), 7.42-7.60 (m, 8H). MS m/z 208 (M+ calcd. for C15H12O=208.3).

Provenance & Evidence

DOI	10.6084/m9.figshare.5104873.v1
Patent number	US06605628B1
Source dataset	uspto-grants-2003_08
ORD ID	ord-99efa8bbbe2c4a429be5355bfd92ca6d
Source note	uspto-grants-2003_08