HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl iodide → HCID 22678040, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | HCID 10298472 | HCID 10298472 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 22678040 | HCID 22678040 | — |
Reaction Steps
5-[5-(4-Chlorophenyl)pent-4-ynyl]-5-(4-methoxybenzenesulfonyl)-thiazolidine-2,4-dione (Example 100) is reated with sodium hydride in DMF, followed by methyl iodide to give the title compound as colorless crystals, mp 113-115° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06605628B1 |
| Source dataset | uspto-grants-2003_08 |
| ORD ID | ord-da9c5956f5e645b1aa7fe7904acce195 |
| Source note | uspto-grants-2003_08 |