Ethyl 4-bromobenzoate → HCID 22558010, compound

HRID 395465Notes

Reaction equation

HRID 395465 reaction equation
[CH3:1][O:2][C:3]1[CH:4]=[C:5](B(O)O)[CH:6]=[C:7]([O:11][CH3:12])[C:8]=1[O:9][CH3:10].Br[C:17]1[CH:27]=[CH:26][C:20]([C:21]([O:23][CH2:24][CH3:25])=[O:22])=[CH:19][CH:18]=1>>[CH3:1][O:2][C:3]1[CH:4]=[C:5]([C:17]2[CH:27]=[CH:26][C:20]([C:21]([O:23][CH2:24][CH3:25])=[O:22])=[CH:19][CH:18]=2)[CH:6]=[C:7]([O:11][CH3:12])[C:8]=1[O:9][CH3:10]

Participants

3

Reactant 2

HCID 22043Ethyl 4-bromobenzoateHCID 27343903,4,5-Trimethoxybenzeneboronic acid

Product 1

HCID 22558010HCID 22558010, compound

Procedure

3,4,5-Trimethoxyphenylboronic acid (2.01 g) and ethyl 4-bromobenzoate (2.29 g) were condensed in the same manner as described in Preparation Example 1 to give the title compound.

Workup

  1. customcondensed in the same manner
  2. customas described in Preparation Example 1

Sources & evidence

ORD record
ord-d80f3bf5547044a08cf5d4868f65f91a
Source dataset
uspto-grants-2003_08
Patent number
US06605620B1

Reaction notes

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