2-Hydrazinopyridine → HCID 11719333, compound

HRID 39554Notes

Reaction equation

HRID 39554 reaction equation
[F:1][C:2]1[CH:7]=[C:6]([I:8])[CH:5]=[CH:4][C:3]=1[NH:9][C:10]1[CH:18]=[N:17][CH:16]=[CH:15][C:11]=1[C:12]([OH:14])=O.[N:19]1[CH:24]=[CH:23][CH:22]=[CH:21][C:20]=1[NH:25][NH2:26]>>[F:1][C:2]1[CH:7]=[C:6]([I:8])[CH:5]=[CH:4][C:3]=1[NH:9][C:10]1[CH:18]=[N:17][CH:16]=[CH:15][C:11]=1[C:12]([NH:26][NH:25][C:20]1[CH:21]=[CH:22][CH:23]=[CH:24][N:19]=1)=[O:14]

Participants

3

Reactant 2

HCID 786452-HydrazinopyridineHCID 590267913-((2-Fluoro-4-iodophenyl)amino)isonicotinic acid2×

Product 1

HCID 11719333HCID 11719333, compound

Procedure

3-[(2-fluoro-4-iodophenyl)amino]-N′-pyridin-2-ylisonicotinohydrazide was synthesized according to the procedure for General Method 1, outlined above, starting with 0.5 mmol of 3-[(2-fluoro-4-iodophenyl)amino]isonicotinic acid (intermediate 1) and 0.8 mmol of pyridin-2-yl-hydrazine. LC/MS [6.90 min; 450 (M+1)]

Workup

  1. customLC/MS [6.90 min; 450 (M+1)]

Sources & evidence

ORD record
ord-ce33ff6cdcf4458b8e73e898d1d7b990
Source dataset
uspto-grants-2013_09
Patent number
US08524911B2

Reaction notes

Loading…