HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Methylphenylhydrazine monohydrochloride → Ethyl 5-Methyl-2-phenyl-1H-indole-3-butanoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Methylphenylhydrazine monohydrochloride | HCID 12504 | — |
| Reactant | Ethyl 6-oxo-6-phenylhexanoate | HCID 3681727 | — |
| Product | Ethyl 5-Methyl-2-phenyl-1H-indole-3-butanoate | HCID 18175131 | 58% |
Reaction Steps
The expected ester is obtained in the form of a brown solid with a yield of 58% by following a procedure analogous to Preparation X and starting from ethyl ε-oxobenzenehexanoate and 4-methylphenylhydrazine hydrochloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06605633B1 |
| Source dataset | uspto-grants-2003_08 |
| ORD ID | ord-5a414143a9f946b48bfcd6a1f0524824 |
| Source note | uspto-grants-2003_08 |