HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-(Dimethylsulfamoyl)benzoic acid → N1-(4-Methoxybenzoyl)-N2-[4-(dimethylaminosulfonyl)benzoyl]-1,2-benzenediamine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-(Dimethylsulfamoyl)benzoic acid | HCID 14572 | — |
| Reactant | N-(2-Aminophenyl)-4-methoxybenzamide | HCID 785232 | — |
| Product | N1-(4-Methoxybenzoyl)-N2-[4-(dimethylaminosulfonyl)benzoyl]-1,2-benzenediamine | HCID 10789847 | 35% |
Reaction Steps
Using the procedure described in Example 55, Part B, N1-(4-methoxybenzoyl)-1,2-benzenediamine (534 mg, 2.21 mmol) was reacted with 4-(dimethylaminosulfonyl)benzoic acid (534 mg, 2.33 mmol) to yield 349 mg (35%) of the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06605626B2 |
| Source dataset | uspto-grants-2003_08 |
| ORD ID | ord-5e57b4707a5141c781e5f0a0bef918e7 |
| Source note | uspto-grants-2003_08 |