HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Ethylbenzoyl chloride → n1-(4-Methoxybenzoyl)-n2-(4-ethylbenzoyl)-4-(tert-butyldimethylsilyloxy)-1,2-benzenediamine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Ethylbenzoyl chloride | HCID 85368 | — |
| Reactant | N1-(4-methoxybenzoyl)-4-(tert-butyldimethylsilyloxy)-1,2-benzenediamine | HCID 54024338 | — |
| Product | n1-(4-Methoxybenzoyl)-n2-(4-ethylbenzoyl)-4-(tert-butyldimethylsilyloxy)-1,2-benzenediamine | HCID 10577465 | 88.1% |
Reaction Steps
Using the procedure described in Example 68, Part A, N1-(4-methoxybenzoyl)-4-(tert-butyldimethylsilyloxy)-1,2-benzenediamine (300 mg, 0.81 mmol) was reacted with 4-ethylbenzoyl chloride (0.13 mL, 0.89 mmol) to yield 360 mg (88%) of the title compound as a white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06605626B2 |
| Source dataset | uspto-grants-2003_08 |
| ORD ID | ord-c2f6ca8d42f647f6ae0cb93a20c366b7 |
| Source note | uspto-grants-2003_08 |