p-Anisoyl chloride → HCID 21352798, compound

HRID 395742Notes

Reaction equation

HRID 395742 reaction equation
[CH3:1][O:2][C:3]1[CH:4]=[C:5]([NH2:22])[C:6]([NH:9][C:10](=[O:21])[C:11]2[CH:16]=[CH:15][C:14]([C:17]([CH3:20])([CH3:19])[CH3:18])=[CH:13][CH:12]=2)=[CH:7][CH:8]=1.[CH3:23][O:24][C:25]1[CH:33]=[CH:32][C:28]([C:29](Cl)=[O:30])=[CH:27][CH:26]=1>>[C:17]([C:14]1[CH:15]=[CH:16][C:11]([C:10]([NH:9][C:6]2[C:5]([NH:22][C:29](=[O:30])[C:28]3[CH:32]=[CH:33][C:25]([O:24][CH3:23])=[CH:26][CH:27]=3)=[CH:4][C:3]([O:2][CH3:1])=[CH:8][CH:7]=2)=[O:21])=[CH:12][CH:13]=1)([CH3:18])([CH3:19])[CH3:20]

Participants

3

Reactant 2

HCID 7477p-Anisoyl chlorideHCID 1133405HCID 1133405, compound

Product 1

HCID 21352798HCID 21352798, compoundYield 99%

Procedure

Using the procedure described in Example 68, Part A, 4-methoxy-N1-(4-tert-butylbenzoyl)-1,2-benzenediamine (3.35 g, 10.1 mmol) was reacted with 4-methoxybenzoyl chloride to yield 1.45 g (99%) of the title compound as a white solid.

Sources & evidence

ORD record
ord-f062cff326694265b89967096c4c5234
Source dataset
uspto-grants-2003_08
Patent number
US06605626B2

Reaction notes

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