Ethanol → HCID 21352776, compound

HRID 395744Notes

Reaction equation

HRID 395744 reaction equation
[C:1]([C:5]1[CH:30]=[CH:29][C:8]([C:9]([N:11](C(=O)C2C=CC=C(C=O)C=2)[C:12]2[C:13]([NH2:18])=[CH:14][CH:15]=[CH:16][CH:17]=2)=[O:10])=[CH:7][CH:6]=1)([CH3:4])([CH3:3])[CH3:2].[CH2:31]([OH:33])[CH3:32]>>[C:1]([C:5]1[CH:30]=[CH:29][C:8]([C:9]([NH:11][C:12]2[C:13]([NH:18][C:9](=[O:10])[C:8]3[CH:7]=[CH:6][CH:5]=[C:32]([CH2:31][OH:33])[CH:29]=3)=[CH:14][CH:15]=[CH:16][CH:17]=2)=[O:10])=[CH:7][CH:6]=1)([CH3:3])([CH3:4])[CH3:2]

Participants

3

Reactant 2

HCID 702EthanolHCID 53927924HCID 53927924, compound

Product 1

HCID 21352776HCID 21352776, compoundYield 99%

Procedure

Using the procedure described in Example 57, N2-(4-tert-butylbenzoyl)-N2-(3-formylbenzoyl)-1,2-benzenediamine (230 mg, 0.57 mmol) was reacted in ethanol to yield 227 mg (99%) of the title compound as an off-white amorphous solid.

Sources & evidence

ORD record
ord-7675ab7e38f24e4e9a6e362e49ef5578
Source dataset
uspto-grants-2003_08
Patent number
US06605626B2

Reaction notes

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