HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Butanesulfonyl chloride → HCID 18174471, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Butanesulfonyl chloride | HCID 75430 | — |
| Reactant | 4-Amino-2-[[4-(1,1-dimethylethyl)benzoyl]amino]-N-(4-methoxyphenyl)benzamide | HCID 10811899 | — |
| Solvent | Triethylamine | HCID 8471 | — |
| Product | HCID 18174471 | HCID 18174471 | 20% |
Reaction Steps
Using the procedure described in Example 59, Part E, 2-(4-tert-butylbenzoylamino)-4-amino-N-(4-methoxyphenyl)benzamide (500 mg, 1.20 mmol) was reacted with butylsulfonyl chloride in the presence of triethylamine to yield 130 mg (20%) of the title compound as an off-white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06605626B2 |
| Source dataset | uspto-grants-2003_08 |
| ORD ID | ord-34b7ca5d027a4edaa034b195b555714c |
| Source note | uspto-grants-2003_08 |