Benzoyl chloride, 3-nitro- → HCID 53683617, compound

HRID 395781Notes

Reaction equation

HRID 395781 reaction equation
[N+:1]([C:4]1[CH:5]=[C:6]([CH:10]=[CH:11][CH:12]=1)[C:7](Cl)=[O:8])([O-:3])=[O:2].[CH3:13][O:14][C:15]1[CH:30]=[CH:29][C:18]([C:19]([NH:21][C:22]2[C:23]([NH2:28])=[CH:24][CH:25]=[CH:26][CH:27]=2)=[O:20])=[CH:17][CH:16]=1>>[N+:1]([C:4]1[CH:5]=[C:6]([CH:10]=[CH:11][CH:12]=1)[C:7]([NH:28][C:23]1[C:22]([NH:21][C:19](=[O:20])[C:18]2[CH:17]=[CH:16][C:15]([O:14][CH3:13])=[CH:30][CH:29]=2)=[CH:27][CH:26]=[CH:25][CH:24]=1)=[O:8])([O-:3])=[O:2]

Participants

3

Reactant 2

HCID 8495Benzoyl chloride, 3-nitro-HCID 785232N-(2-Aminophenyl)-4-methoxybenzamide

Product 1

HCID 53683617HCID 53683617, compoundYield 86.1%

Procedure

Using the procedure described in Example 93, Part A, 3-nitrobenzoyl chloride (2.3 mmol) and N1-(4-methoxybenzoyl)-1,2-benzenediamine (2.1 mmol) yielded 708 mg (86%) of the title compound.

Sources & evidence

ORD record
ord-03fd7dadb4ed427ba87928a963082889
Source dataset
uspto-grants-2003_08
Patent number
US06605626B2

Reaction notes

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