2-Fluoroaniline → HCID 2223570, compound

HRID 395833Notes

Reaction equation

HRID 395833 reaction equation
[F:1][C:2]1[CH:8]=[CH:7][CH:6]=[CH:5][C:3]=1[NH2:4].[N+:9]([C:12]1[CH:20]=[CH:19][CH:18]=[CH:17][C:13]=1[C:14](Cl)=[O:15])([O-:11])=[O:10]>>[N+:9]([C:12]1[CH:20]=[CH:19][CH:18]=[CH:17][C:13]=1[C:14]([NH:4][C:3]1[CH:5]=[CH:6][CH:7]=[CH:8][C:2]=1[F:1])=[O:15])([O-:11])=[O:10]

Participants

3

Reactant 2

HCID 95842-FluoroanilineHCID 118752-Nitrobenzoyl chloride

Product 1

HCID 2223570HCID 2223570, compoundYield 70.2%

Procedure

Using the procedure described in Example 93, Part A, 2-fluoroaniline (20.7 mmol) and 2-nitrobenzoyl chloride (22.8 mmol) yielded 3.78 g (70%) of the title compound.

Sources & evidence

ORD record
ord-3d2eddde78944c8e82cba1ef56f18c04
Source dataset
uspto-grants-2003_08
Patent number
US06605626B2

Reaction notes

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