3-Chloroaniline → N-(3-Chlorophenyl)-2-nitrobenzamide

HRID 395837Notes

Reaction equation

HRID 395837 reaction equation
[Cl:1][C:2]1[CH:3]=[C:4]([CH:6]=[CH:7][CH:8]=1)[NH2:5].[N+:9]([C:12]1[CH:20]=[CH:19][CH:18]=[CH:17][C:13]=1[C:14](Cl)=[O:15])([O-:11])=[O:10]>>[N+:9]([C:12]1[CH:20]=[CH:19][CH:18]=[CH:17][C:13]=1[C:14]([NH:5][C:4]1[CH:6]=[CH:7][CH:8]=[C:2]([Cl:1])[CH:3]=1)=[O:15])([O-:11])=[O:10]

Participants

3

Reactant 2

HCID 79323-ChloroanilineHCID 118752-Nitrobenzoyl chloride

Product 1

HCID 720053N-(3-Chlorophenyl)-2-nitrobenzamideYield 98%

Procedure

Using the procedure described in Example 93, Part A, 3-chloroaniline (9.4 mmol) and 2-nitrobenzoyl chloride (10.4 mmol) yielded 2.55 g (98%) of the title compound.

Sources & evidence

ORD record
ord-d27afe1e94c54d0b910927cf72e0b2d1
Source dataset
uspto-grants-2003_08
Patent number
US06605626B2

Reaction notes

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