4-(Dimethylamino)benzoic acid → HCID 10786568, compound

HRID 395851Notes

Reaction equation

HRID 395851 reaction equation
[CH3:1][N:2]([CH3:12])[C:3]1[CH:11]=[CH:10][C:6]([C:7]([OH:9])=O)=[CH:5][CH:4]=1.[NH2:13][C:14]1[CH:30]=[CH:29][CH:28]=[CH:27][C:15]=1[C:16]([NH:18][C:19]1[CH:24]=[CH:23][C:22]([O:25][CH3:26])=[CH:21][CH:20]=1)=[O:17]>>[CH3:12][N:2]([CH3:1])[C:3]1[CH:4]=[CH:5][C:6]([C:7]([NH:13][C:14]2[CH:30]=[CH:29][CH:28]=[CH:27][C:15]=2[C:16]([NH:18][C:19]2[CH:20]=[CH:21][C:22]([O:25][CH3:26])=[CH:23][CH:24]=2)=[O:17])=[O:9])=[CH:10][CH:11]=1

Participants

3

Reactant 2

HCID 120924-(Dimethylamino)benzoic acidHCID 4788202-amino-N-(4-methoxyphenyl)benzamide

Product 1

HCID 10786568HCID 10786568, compoundYield 91%

Procedure

Using the procedure described in Example 55, Part B, 4-dimethylaminobenzoic acid and 2-amino-N-(4-methoxyphenyl)benzamide (1.25 mmol), yielded 444 mg (91%) of the title compound as a white solid.

Sources & evidence

ORD record
ord-c0972a24aebc4d11ae54ef3b8227eff1
Source dataset
uspto-grants-2003_08
Patent number
US06605626B2

Reaction notes

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