HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 18173088, compound → HCID 18173048, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 18173088 | HCID 18173088 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 18173048 | HCID 18173048 | — |
Reaction Steps
3-Benzyloxymethyl-5-(2,6-dioxo-1,3-dipropyl-2,3,6,7-tetrahydro-1H-purin-8-yl)-tricyclo[2.2.1.02,6]heptane-3-carboxylic acid (50 mg) was hydrogenated in ethyl acetate using Pd/C 5% under 1 atm of H2 overnight. The catalyst was filtered through silica eluting with 10% MeOH:CHCl3. Yield 31 mg. Mass (ES+ 403).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06605600B1 |
| Source dataset | uspto-grants-2003_08 |
| ORD ID | ord-8cf4250484ea4bb3a1cdbdcd13e74685 |
| Source note | uspto-grants-2003_08 |