Sodium Bicarbonate → HCID 18173103, compound

Participants

Reaction Steps

The product (390 mg) from Example 35, was taken in THF (10 ml) 6N HCl (3 ml) and heated to reflux overnight. The next day, after cooling to room temperature, poured over ice, neutralized with NaHCO3, extracted with ethyl acetate, washed with brine and dried over MgSO4. Filtered, concentrated, and purified on silica. Yield (321 mg). Mass (ES+ 359).

Provenance & Evidence