1-Butanol → HCID 22218522, compound

HRID 395920Notes

Reaction equation

HRID 395920 reaction equation
[C:1]([O:5][CH2:6][CH2:7][CH2:8][CH3:9])(=[O:4])[CH:2]=[CH2:3].C(O)CCC>O>[CH2:6]([OH:5])[CH2:7][CH2:8][CH3:9].[C:1]([O:5][CH2:6][CH2:7][CH2:8][CH3:9])(=[O:4])[CH:2]=[CH2:3]

Participants

4

Reactant 2

HCID 2631-ButanolHCID 8846Butyl Acrylate2×

Product 1

HCID 22218522HCID 22218522, compound

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

U.S. Pat. No. 4,280,010 discloses a process for making butyl acrylate in which the reaction overhead is passed to a reactor column with the distillate being a butyl acrylate, butanol and water azeotrope. A reflux is used in the reactor column. The remainder of the distillate is sent to a dehydration column and the organic product is further distilled to provide a butanol—butyl acrylate azeotrope being recycled to the reactor and butyl acrylate stream being obtained at the base of the column.

Workup

  1. customis passed to a reactor
  2. distillationthe organic product is further distilled

Sources & evidence

ORD record
ord-50390dffc4d04b1da79e89c15c526e4f
Source dataset
uspto-grants-2003_08
Patent number
US06605738B1

Reaction notes

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