HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 69985584, compound → HCID 10302914, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 69985584 | HCID 69985584 | — |
| Solvent | Chloroform methanol | HCID 21584188 | — |
| Product | HCID 10302914 | HCID 10302914 | 47.5% |
Reaction Steps
4-[4-(2-{[(2S)-3-(4-{[tert-Butyl(diphenyl)silyl]oxy}phenoxy)-2-hydroxy-propyl]amino}ethyl)anilino]-N-(3,5-difluorobenzyl)-1-piperidinecarboxamide (0.165 g, 0.20 mmol) was reacted according to Procedure H (eluant: 5:1 chloroform-methanol containing 1% ammonium hydroxide) to give the title compound (0.05 g, 0.095 mmol)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06605618B2 |
| Source dataset | uspto-grants-2003_08 |
| ORD ID | ord-70b8b0e265e54be384325cab757a7a63 |
| Source note | uspto-grants-2003_08 |