HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 69985889, compound → HCID 10209574, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 69985889 | HCID 69985889 | — |
| Solvent | Chloroform methanol | HCID 21584188 | — |
| Product | HCID 10209574 | HCID 10209574 | 44.8% |
Reaction Steps
4-[4-(2-{[(2S)-3-(4-{[tert-Butyl (diphenyl)silyl]oxy}phenoxy)-2-hydroxypropyl]amino}ethyl)anilino]-N-(2,5-difluorobenzyl)-1-piperidinecarboxamide (0.238 g, 0.29 mmol) was reacted according to Procedure H (eluant: 5:1 chloroform-methanol containing 1% ammonium hydroxide) to give the title compound (0.075 g, 0.13 mmol).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06605618B2 |
| Source dataset | uspto-grants-2003_08 |
| ORD ID | ord-d1e03376987d4dd7a05fe9f57b97f0f2 |
| Source note | uspto-grants-2003_08 |