HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 69987474, compound → HCID 70002120, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 69987474 | HCID 69987474 | — |
| Solvent | Chloroform methanol | HCID 21584188 | — |
| Product | HCID 70002120 | HCID 70002120 | 68.4% |
Reaction Steps
4-[4-(2-{[(2S)-3-(4-{[tert-Butyl(diphenyl)silyl]oxy}phenoxy)-2-hydroxy-propyl]amino}ethyl)anilino]-N-(3-cyclohexylpropyl)-1-piperidinecarboxamide (0.23 g, 0.291 mmol) was reacted according to Procedure H (eluant: 10:1 going to 5:1 chloroform-methanol containing 2% triethylamine) to give the title compound (0.11 g, 0.199 mmol).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06605618B2 |
| Source dataset | uspto-grants-2003_08 |
| ORD ID | ord-33a9dcadbd2e4350984d8a6edff49dd2 |
| Source note | uspto-grants-2003_08 |