Water → HCID 23003407, compound

Participants

Reaction Steps

A solution of (2-benzoyl-6-chloro-1H-indol-3-yl)acetic acid (Example 2, 200 mg, 0.64 mmol), diethyl phosphorocyanidate (DEPC, 0.12 ml, 0.76 mmol) and triethylamine (0.11 ml, 0.76 mmol) in DMF (3.0 ml) was stirred at room temperature for 5 min. The mixture was then poured into water (20 ml) and the orange precipitates were collected by filtration to give 20 mg (11%) of the title compound as orange solids.

Provenance & Evidence