p-Chlorophenacyl bromide → HCID 23003226, compound

HRID 396510Notes

Reaction equation

HRID 396510 reaction equation
[CH3:1][C:2]1[CH:13]=[CH:12][C:5](/[CH:6]=[CH:7]/[C:8]([O:10][CH3:11])=[O:9])=[C:4]([NH:14]S(C2C=CC=CC=2)(=O)=O)[CH:3]=1.[Cl:24][C:25]1[CH:34]=[CH:33][C:28]([C:29](=[O:32])[CH2:30]Br)=[CH:27][CH:26]=1>>[CH3:11][O:10][C:8](=[O:9])[CH2:7][C:6]1[C:5]2[C:4](=[CH:3][C:2]([CH3:1])=[CH:13][CH:12]=2)[NH:14][C:30]=1[C:29](=[O:32])[C:28]1[CH:33]=[CH:34][C:25]([Cl:24])=[CH:26][CH:27]=1

Participants

3

Reactant 2

HCID 68303p-Chlorophenacyl bromideHCID 23003315HCID 23003315, compound

Product 1

HCID 23003226HCID 23003226, compound

Procedure

The title compound was prepared according to the procedure described in Example 57 from methyl trans-4-methyl-2-(phenylsulfonylamino)cinnamate (step 2 of Example 149) and 4-chlorophenacyl bromide.

Sources & evidence

ORD record
ord-855928abf3d94bf3b96136ef288d0426
Source dataset
uspto-grants-2003_08
Patent number
US06608070B1

Reaction notes

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