2-Bromo-4'-nitroacetophenone → HCID 23003509, compound

HRID 396519Notes

Reaction equation

HRID 396519 reaction equation
[Cl:1][C:2]1[CH:13]=[CH:12][C:5](/[CH:6]=[CH:7]/[C:8]([O:10][CH3:11])=[O:9])=[C:4]([NH:14]S(C2C=CC=CC=2)(=O)=O)[CH:3]=1.[N+:24]([C:27]1[CH:36]=[CH:35][C:30]([C:31](=[O:34])[CH2:32]Br)=[CH:29][CH:28]=1)([O-:26])=[O:25]>>[CH3:11][O:10][C:8](=[O:9])[CH2:7][C:6]1[C:5]2[C:4](=[CH:3][C:2]([Cl:1])=[CH:13][CH:12]=2)[NH:14][C:32]=1[C:31](=[O:34])[C:30]1[CH:29]=[CH:28][C:27]([N+:24]([O-:26])=[O:25])=[CH:36][CH:35]=1

Participants

3

Reactant 2

HCID 668402-Bromo-4'-nitroacetophenoneHCID 11371593Methyl trans-4-chloro-2-(phenylsulfonylamino)cinnamate

Product 1

HCID 23003509HCID 23003509, compound

Procedure

The title compound was prepared according to the procedure described in Example 57 from methyl trans 4-chloro-2-(phenylsulfonylamino)cinnamate (step 1 of Example 8, Method A) and 4-nitrophenacyl bromide.

Sources & evidence

ORD record
ord-dc72180033cc417faa04ce60762dd520
Source dataset
uspto-grants-2003_08
Patent number
US06608070B1

Reaction notes

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