3-Chloro-4-methanesulfonylaniline → 3-Hydroxymethyl-4-(methylsulfonyl)phenylhydrazine hydrochloride

HRID 396813Notes

Reaction equation

HRID 396813 reaction equation
[OH:1][CH2:2][C:3]1[CH:4]=[C:5]([CH:7]=[CH:8][C:9]=1[S:10]([CH3:13])(=[O:12])=[O:11])[NH2:6].[Cl:14]C1C=C(C=CC=1S(C)(=O)=O)[NH2:18]>>[ClH:14].[OH:1][CH2:2][C:3]1[CH:4]=[C:5]([NH:6][NH2:18])[CH:7]=[CH:8][C:9]=1[S:10]([CH3:13])(=[O:12])=[O:11]

Participants

3

Reactant 2

HCID 108459213-Chloro-4-methanesulfonylanilineHCID 223166243-Hydroxymethyl-4-(methylsulfonyl)aniline

Product 1

HCID 223167563-Hydroxymethyl-4-(methylsulfonyl)phenylhydrazine hydrochloride

Procedure

The title compound was prepared according to the procedure of step 1 of Example 155 using 3-hydroxymethyl-4-(methylsulfonyl)aniline from step3 instead of 3-chloro-4-(methylsulfonyl)aniline.

Sources & evidence

ORD record
ord-616e8c83630f46f794c20565ad2a4339
Source dataset
uspto-grants-2003_08
Patent number
US06608095B2

Reaction notes

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