HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thioacetamide → HCID 22316705, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thioacetamide | HCID 2723949 | — |
| Reactant | HCID 53712477 | HCID 53712477 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 22316705 | HCID 22316705 | 56.1% |
Reaction Steps
A mixture of 2-bromo-2-(4-bromophenyl)-1-(4-methylthiophenyl)ethanone (7.6 g, 0.018 mol) and thioacetamide 1.4 g, 0.018 mol) in ethanol (150 mL) was refluxed for 1 day. The mixture was concentrated and the solid was purified by flash chromatography eluting with CH2Cl2/hexane (2/1) to give title compound (3.8 g, 56%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06608095B2 |
| Source dataset | uspto-grants-2003_08 |
| ORD ID | ord-fae6855e416f4961947f5af682900102 |
| Source note | uspto-grants-2003_08 |