HuagongsheHuagongshe Chemistry Print Report · For research reference only
p-Toluenesulfonic acid → Diisobutylaluminum hydride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | p-Toluenesulfonic acid | HCID 6101 | — |
| Reactant | Phenazopyridine hydrochloride | HCID 8691 | — |
| Reactant | tert-Butyldimethylsilyl chloride | HCID 28928 | — |
| Reactant | HCID 22034396 | HCID 22034396 | — |
| Reactant | HCID 178418287 | HCID 178418287 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | Diisobutylaluminum hydride | HCID 14487 | — |
Reaction Steps
diisobutoxyaluminum hydride, pTsOH: p-toluenesulphonic acid, MeOH: methanol, CITBS: chloro-dimethyl-t-butyl silane, PCC: pyridium chlorochrome, W-K: Wolff-Kishiner reduction.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06608215B2 |
| Source dataset | uspto-grants-2003_08 |
| ORD ID | ord-7f5340b852f3480c8a70a2fbafd9f35a |
| Source note | uspto-grants-2003_08 |