反应详情

After completion of the reaction, the reaction mixture was diluted with water and extracted with ether. The extract was dried over magnesium sulfate. The solvent was distilled off to obtain 24.2 g (yield: 94.8%) of bis(3-hydroxypropyl)diphenylsilane (B) (m.p. 80°-81° C.).

1. customAfter completion of the reaction
2. extractionextracted with ether
3. dry with materialThe extract was dried over magnesium sulfate
4. distillationThe solvent was distilled off