Bis(3-hydroxypropyl)diphenylsilane → HCID 15606542, compound

HRID 3972Notes

Reaction equation

HRID 3972 reaction equation
[OH:1][CH2:2][CH2:3][CH2:4][Si:5]([CH2:18][CH2:19][CH2:20][OH:21])([C:12]1[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=1)[C:6]1[CH:11]=[CH:10][CH:9]=[CH:8][CH:7]=1>O>[C:2]([O:1][CH2:2][CH2:3][CH2:4][Si:5]([CH2:18][CH2:19][CH2:20][O:21][C:20](=[O:21])[CH:19]=[CH2:18])([C:12]1[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=1)[C:6]1[CH:11]=[CH:10][CH:9]=[CH:8][CH:7]=1)(=[O:1])[CH:3]=[CH2:4]

Participants

3

Reactant 1

HCID 15606541Bis(3-hydroxypropyl)diphenylsilane

Product 1

HCID 15606542HCID 15606542, compound

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

After completion of the reaction, the reaction mixture was diluted with water and extracted with ether. The extract was dried over magnesium sulfate. The solvent was distilled off to obtain 24.2 g (yield: 94.8%) of bis(3-hydroxypropyl)diphenylsilane (B) (m.p. 80°-81° C.).

Workup

  1. customAfter completion of the reaction
  2. extractionextracted with ether
  3. dry with materialThe extract was dried over magnesium sulfate
  4. distillationThe solvent was distilled off

Sources & evidence

ORD record
ord-c7d8e13ae3ae4861ac0b9cc8bcfa101e
Source dataset
uspto-grants-1988_02
Patent number
US04723025

Reaction notes

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