反应详情

温度

65 °C

To a 1 L Morton flask was added diallylmethylamine (86.1 g), 1,10-dibromodecane (112 g), and methanol (100 mL). The mixture was heated to 65° C. for 24 h, and then allowed to cool to room temperature. The solvent was removed by rotary vacuum evaporation. Diethylether (400 mL) was added and the mixture was stirred for 1 hr. The mixture was allowed to settle and the top layer was decanted and discarded. The remaining oil was dried by rotary vacuum evaporation to yield 215 g of product.

1. temperatureto cool to room temperature
2. customThe solvent was removed by rotary vacuum evaporation
3. additionDiethylether (400 mL) was added
4. customthe top layer was decanted
5. customThe remaining oil was dried by rotary vacuum evaporation