HuagongsheHuagongshe Chemistry Print Report · For research reference only
Oxalyl chloride → HCID 57035411, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Oxalyl chloride | HCID 65578 | — |
| Reactant | HCID 975442 | HCID 975442 | — |
| Product | HCID 57035411 | HCID 57035411 | — |
Reaction Steps
The title compound was prepared by a similar method to Preparation 3 from (2S)-1-[(4-fluorophenyl)sulfonyl]-2-pyrrolidinecarboxamide [see Preparation 50] and oxalyl chloride. The crude product was purified by column chromatography on silica gel eluting with dichloromethane to afford (2S)-1-[(4-fluorophenyl)sulfonyl]-2-pyrrolidinecarbonitrile as a white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06610707B1 |
| Source dataset | uspto-grants-2003_08 |
| ORD ID | ord-d8441bc1a298499bb6a89aefc59a963e |
| Source note | uspto-grants-2003_08 |