HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrazine → HCID 508587, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrazine | HCID 9321 | — |
| Reactant | HCID 508581 | HCID 508581 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 508587 | HCID 508587 | 60% |
Reaction Steps
A portion of the crude intermediate of example 58 above, (50 mg, 0.06 mmol) was added to a solution of hydrazine in ethanol (1M, 10 mL). The resulting solution was stirred for 3 h before evaporation of the solvent. The residue was purified by preparative HPLC to yield 25 mg, 60% of the desired material.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06610689B2 |
| Source dataset | uspto-grants-2003_08 |
| ORD ID | ord-02def1a14a4d46faa537fc6bae46c121 |
| Source note | uspto-grants-2003_08 |