HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Methylimidazole → HCID 23444999, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Methylimidazole | HCID 12749 | — |
| Reactant | HCID 23444948 | HCID 23444948 | — |
| Product | HCID 23444999 | HCID 23444999 | — |
Reaction Steps
The title compound, MS: m/e=292.2 (M+H+) was obtained as a beige solid (77% yield) by the reaction of 3-chloromethyl-5-(3,4-dimethyl-phenyl)-2-methyl-pyridine hydrochloride (1:1) with 2-methylimidazole (5 eq.), using sodium hydride (3 eq.) as base followed by formation of the hydrochloride salt.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06610723B2 |
| Source dataset | uspto-grants-2003_08 |
| ORD ID | ord-5e24843e8c1648e1910a72cb37f74610 |
| Source note | uspto-grants-2003_08 |